1. Key Laboratory of Food and Drug Safety Prevention and Control in Shanxi Province, Shanxi Provincial Inspection and Testing Centre, Taiyuan 030025, China
2. Department of Chemistry, Changzhi University, Changzhi 046011, China
随着全球农业生产的快速发展和食品贸易的增加,农药残留问题已成为全球食品安全领域的主要挑战之一。世界卫生组织(World Health Organization,WHO)和联合国粮农组织(Food and Agriculture Organization of the United Nations,FAO)指出,农药残留的管理和控制对于确保食品安全和减少公共健康风险至关重要[1-2]。在众多农药中,噁唑菌酮由于杀菌效果好,单剂和复配制剂等新品种在我国不断登记上市,使用量逐年增加,广泛应用于葡萄、西红柿、马铃薯等作物上。此外,葡萄作为一种高附加值的经济作物,具有较高的农药使用率和残留风险,因此选择葡萄中噁唑菌酮农药残留作为本文研究对象具有重要的现实意义。
GERAGEJ M, MEIRAA P G, SILVA M VDA. Food and Nutrition Security: Pesticide Residues in Food[J]. Nutrire, 2017, 42(3): 3-9. DOI:10.1186/s41110-016-0028-4 .
[2]
VAN DEN BERGH, GUB G, GRENIERB, et al. Pesticide Lifecycle Management in Agriculture and Public Health: Where Are the Gaps?[J]. Sci Total Environ, 2020, 742: 140598. DOI:10.1016/j.scitotenv.2020.140598 .
[3]
POSSOLOA. Five Examples of Assessment and Expression of Measurement Uncertainty[J]. Appl Stoch Models Bus Ind, 2013, 29(1): 1-18. DOI:10.1002/asmb.1947 .
ZHAIH W, FANS F, WANGJ, et al. Recent Progress in Measurement Uncertainty and Its Application in Food Inspection and Detection[J]. Food Sci, 2021, 42(5): 314-320. DOI: 10.7506/spkx1002-6630-20200226-287 .
[6]
VON CLARMANNT, COMPERNOLLES, HASEF. Truth and Uncertainty. A Critical Discussion of the Error Concept Versus the Uncertainty Concept[J]. Atmos Meas Tech, 2022, 15(5): 1145-1157. DOI:10.5194/amt-15-1145-2022 .
[7]
SUNR, YANGW Q, LIY X, et al. Multi-residue Analytical Methods for Pesticides in Teas: A Review[J]. Eur Food Res Technol, 2021, 247(8): 1839-1858. DOI:10.1007/s00217-021-03765-3 .
[8]
PENGB, XIEY L, LAIQ F, et al. Pesticide Residue Detection Technology for Herbal Medicine: Current Status, Challenges, and Prospects[J]. Anal Sci, 2024, 40(4): 581-597. DOI:10.1007/s44211-024-00515-9 .
LIJ, CAIT, DAIH J, et al. Evaluation of Measurement Uncertainty for the Determination of Pyridaben and Other Nine Pesticide Residues in Tea by Gas Chromatography-mass Spectrometry[J]. Sci Technol Food Ind, 2022, 43(14): 311-322. DOI: 10.13386/j.issn1002-0306.2021090073 .
General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China. Evaluation of Uncertainty in Chemical Analysis Measurement: JJF 1135-2005 [S]. Beijing: Metrology Publishing House, 2005.
General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China. Evaluation and Expression of Uncertaintv in Measurement: JJF 1059.1-2012 [S]. Beijing: Standards Press of China, 2013.
YANGY C, ZHENGC L, LIUX, et al. Evaluation of Uncertainty in Determination of Dimethomorph Residue in Strawberry by QuEChERS-liquid Chromatography-tandem Mass Spectrometry Method[J]. Agrochemicals, 2022, 61(2): 127-131. DOI: 10.16820/j.cnki.1006-0413.2022.02.012 .
LIQ. Measurement Uncertainty and Quality Judgement of Determination of Pesticide Residue in Vegetable with Gas Chromatography[J]. J Yulin Univ, 2020, 30(6): 32-37. DOI: 10.16752/j.cnki.jylu.2020.06.007 .
WEIW J, WANGL F. Evaluation of Measurement Uncertainty in Determination of Carbofuran Residue in Chilli by Liquid Chromatography[J]. J Anhui Agric Sci, 2015, 43(8): 89-91. DOI: 10.13989/j.cnki.0517-6611.2015.08.035 .
LINJ X, LINQ, CHIH. Discussion on Several Problems in Evaluation of Measurement Uncertainty[J]. China Metrol, 2018(11): 81-85. DOI: 10.16569/j.cnki.cn11-3720/t.2018.11.033 .
ZHAOK, ZHUOQ X, ZHANGM J, et al. Some Ideas of Uncertainty in Chemical Analysis Measurement[J]. China Insp Body Lab, 2023, 31(4): 53-56. DOI: 10.16428/j.cnki.cn10-1469/tb.2023.04.014 .
WANGJ Y, ZHANGR Q, XUL X, et al. Several Confusing Problems in the Evaluation of Measurement Uncertainty[J]. Chin J Health Stat, 2010, 27(5):552-553. DOI:10.3969/j.issn.1002-3674.2010.05.035 .
LIUF. Understanding of Several Problems in Evaluation of Measurement Uncertainty[J]. China Metrol, 2015(9): 100-101. DOI: 10.16569/j.cnki.cn11-3720/t.2015.09.057 .
General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China. Verification Regulation for Electronic Balance: JJG 1036-2008 [S]. Beijing: China Quality Inspection Press, 2008.
ZHAOC Y, RENL L, PUC, et al. Measurement and Uncertainty Evaluation of Fullerene Purity Based on Ultraviolet-visible Spectrophotometer[J]. Acta Metrol Sin, 2023, 44(12): 1904-1911. DOI: 10.3969/j.issn.1000-1158.2023.12.17 .
LIANGJ Y, ZHANGZ Z, LIANGL Y, et al. Uncertainty Evaluation for Determination of Benzoic Acid and Sorbic Acid in Fruit Leather by HPLC[J]. Yunnan Chem Technol, 2022, 49(11): 56-61. DOI: 10.3969/j.issn.1004-275X.2022.11.15 .
DINGS M, CAIQ D, XIAB. Evaluationof the Uncertainty in Determination of Chloramphenicol in Fish by UPLC-MS/MS[J]. Shandong Chem Ind, 2021, 50(12): 96-99. DOI: 10.19319/j.cnki.issn.1008-021x.2021.12.031 .
General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China. Verification Regulation of Working Glass Container: JJG 196-2006 [S]. Beijing: China Metrology Publishing House, 2007.
WUK, LIUL T, WEIN G, et al. Evaluation of Uncertainty in Determination of Omethoate Pesticide Residues in Tea by Liquid Chromatography-mass Spectrometry[J]. Farm Prod Process, 2023(13): 64-67. DOI: 10.16693/j.cnki.1671-9646(X).2023.07.016 .
YUT T, QIUP C, CHENQ, et al. Evaluation of the Uncertainty in Determining Organophosphorus and Pyrethroid Pesticides Residue in Vegetables and Fruits by Gas Chromatography[J]. Chin Agric Sci Bull, 2021, 37(17): 129-136.
General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China. Verification Regulation of Locomotive Pipette: JJG 646-2006 [S]. Beijing: China Metrology Publishing House, 2007.
LIJ, ZHANGJ Z, YUX J, et al. Evaluation of Uncertainty in Determination of Plant Growth Regulator Residues in Bean Sprouts by Ultra Performance Liquid Chromatography-tandem Mass Spectrometry[J]. Food Sci, 2019, 40(10): 292-297. DOI: 10.7506/spkx1002-6630-20180323-304 .
ZHAOJ N, ZHAOY, WANGX Y, et al. Evaluation of Uncertainty in Determination of Profenofos by LC-MS[J]. J Salt Sci Chem Ind, 2022, 51(10): 38-42. DOI: 10.16570/j.cnki.issn1673-6850.2022.10.007 .
YANGJ L, LINS T. Uncertainty Analysis of Diazepam Residues by Liquid Chromatography-tandem Mass Spectrometry[J]. China Food Saf Mag, 2023(1): 114-117. DOI: 10.16043/j.cnki.cfs.2023.01.066 .
GAOY K, CHENX M, CHENC Q, et al. Uncertainty Evaluation of Determination of 4 Kinds of Tetracyclines Antibiotics in Tilapia by HPLC-MS/MS[J]. China Food Saf Mag, 2022(32): 97-101. DOI: 10.16043/j.cnki.cfs.2022.32.041 .
ZHOUF J, HUR L, HUANGF, et al. Uncertainty Evaluation and Application of Determination of Chlorpyrifos in Vegetables by GC-MS[J]. Seed Sci Technol, 2022, 40(23): 18-21. DOI: 10.19904/j.cnki.cn14-1160/s.2022.23.006 .
SUNJ W. Uncertainty Evaluation for the Determination of Bifenthrin Residues in Celery by GC-MS/MS[J]. China Food Saf Mag, 2022(34): 55-57. DOI: 10.16043/j.cnki.cfs.2022.34.063 .